Spectrophotometric simultaneous analysis of analgin - Adamon mixture in injection preparations


Acar N., ONUR F.

Analytical Letters, vol.29, no.5, pp.763-773, 1996 (SCI-Expanded, Scopus)

  • Publication Type: Article / Article
  • Volume: 29 Issue: 5
  • Publication Date: 1996
  • Doi Number: 10.1080/00032719608001782
  • Journal Name: Analytical Letters
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.763-773
  • Keywords: Adamon, Analgin, Pharmaceutical preparation, Spectrophotometry
  • Lokman Hekim University Affiliated: No

Abstract

A new method is described for analyzing a binary mixture of analgin and adamon using extractive and derivative spectrophotometry. In the method, analgin and adamon both were extracted into chloroform as an ion-pair with thymol blue from their aqueous solution buffered to pH 3.6. Determination of these drugs was performed by reading the dA/dλ values at 600.0 nm and 310 5 nm in the first derivative spectra of the chloroform layer. Relative standard deviations of the method are 0.10 % for analgin and 0 81 % for adamon. The method was successfully applied to an injection solution containing these two active ingredients.